Navegando por Palavras-chave "Curva Mestre De Sinterização"

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    Investigação Da Cinética De Sinterização De Cerâmicas De (K0,48na0,52)Nbo3 (Knn) Densificadas Por Spark Plasma Sintering
    (Universidade Federal de São Paulo (UNIFESP), 2018-03-29) Souza, Camila Alves De [UNIFESP]; Lente, Manuel Henrique [UNIFESP]; Universidade Federal de São Paulo (UNIFESP)
    In This Work, It Was Proposed The Study Of The Densification Of Lead-Free Piezoelectric Ceramics Based On (Kx,Na1-X)Nbo3 Via Spark Plasma Sintering And The Study Of Sintering Kinetics Through The Determination Of The Master Sintering Curve. In Addition, The Effect Of The Cuo Doping On Knn Properties And The Effect Of A Lower Pressure Applied During The Sintering Process Were Analyzed In A Complementary Manner. Thus, For The Initial Study, Ceramic Samples Of Knn Were Sintered At Different Heating Rates Using The Same Sintering Temperature And Applying The Maximum Allowable Pressure. Then, This Same Criterion Was Applied For Knn Samples Differing Only In The Magnitude Of The Pressure Applied During The Sintering, Whose Value Became The Minimum Allowed. Subsequently, Using The Initial Sintering Parameters, Knn Ceramics Doped With 1.5 %Mol Cuo Were Produced. The Results Were Correlated With Microstructural, Structural And Electrical Properties In Order To Analyze The Influence Of The Sintering Rate, Doping And Di