Browsing by Subject "Mass spectrometry"

Análise do perfil metabolômico do líquido folicular de pacientes com síndrome dos ovários policísticos submetidas ao tratamento de fertilização in vitro

Cordeiro, Fernanda Bertuccez [UNIFESP] (Universidade Federal de São Paulo (UNIFESP), 2017-03-28)

Objectives: Analyze the metabolomic profile of follicular fluid from patients with and without hyper response to controlled ovarian stimulation, associated or not with polycystic ovary syndrome (PCOS). Method: Follicular ...

Application of electrospray ionization mass spectrometry fingerprinting associated with macroscopic and histological analysis for Plantago major herbal infusions quality control

Andrade, Carolina Gomes de; Mesquita, Leonardo Mendes de Souza [UNIFESP]; Murador, Daniella Carisa [UNIFESP]; Braga, Anna Rafaela Cavalcante [UNIFESP]; Rosso, Veridiana Vera de [UNIFESP]; Almeida, Odair Jose Garcia de; Vilegas, Wagner (Elsevier Science Bv, 2018)

The present study demonstrates the need to conduct an integrative quality control of teas marketed as Plantago major. In the present study, quality control checks were performed through macroscopic, microscopic and chemical ...

Automated determination of venlafaxine in human plasma by on-line SPE-LC-MS/MS. Application to a bioequivalence study

Suenaga, Eunice Mayumi [UNIFESP]; Ifa, Demian R.; Cruz, Alessandro Carvalho; Pereira, Renata; Abib, Eduardo; Tominga, Mineko; Nakaie, Clovis Ryuichi [UNIFESP] (Wiley-Blackwell, 2009-02-01)

A new automated SPE-LC-ESI-MS/MS method was developed and validated to quantify venlafaxine in human plasma using fluoxetine as an internal standard. the analytes were automatically extracted from plasma by C18 SPE cartridges, ...

Caracterização da presença de AKT no núcleo de células de melanoma e identificação de proteínas associadas por espectrometria de massas

Coa, Larissa Leggieri [UNIFESP] (Universidade Federal de São Paulo, 2016-08-16)

The serine threonine kinase AKT/PKB is a critical regulator of various essential physiological cellular processes including cell proliferation, survival, motility and size, metabolism and differentiation. Deregulation of ...

Differential cytotoxic effects on odontoblastic cells induced by self-adhesive resin cements as a function of the activation protocol

Perlatti D'Alpino, Paulo Henrique; Moura, Gioconda Emanuella Diniz de Dantas [UNIFESP]; de Arruda Barbosa, Silvana Coelho; Marques, Lygia de Azevedo; Eberlin, Marcos Nogueira; Nascimento, Fabio Dupart; Tersariol, Ivarne Luis dos Santos [UNIFESP] (Elsevier Sci Ltd, 2017)

Objectives. To evaluate the cytotoxic effects of exposing odontoblast cells to a variety of commercial self-adhesive cements polymerized using different activation modes. Methods. Five cements: MaxCem Elite (MAX), Bifix ...

Efficient and eco-friendly synthesis of iodinated aromatic building blocks promoted by iodine and hydrogen peroxide in water: a mechanistic investigation by mass spectrometry

Gallo, Rafael D. C.; Ferreira, Irlon M.; Casagrande, Gleison A.; Pizzuti, Lucas; Oliveira-Silva, Diogo [UNIFESP]; Raminelli, Cristiano [UNIFESP] (Elsevier B.V., 2012-10-03)

The reaction of aromatic and heteroaromatic compounds with molecular iodine in the presence of aqueous hydrogen peroxide using water without any co-solvent at 50 degrees C for 24 h produced versatile iodinated organic ...