Use of spin label EPR spectra to monitor peptide chain aggregation inside resin beads.

Use of spin label EPR spectra to monitor peptide chain aggregation inside resin beads.

Autor Cilli, E. M. Google Scholar
Marchetto, R. Google Scholar
Schreier, S. Google Scholar
Nakaie, C. R. Google Scholar
Instituição UNESP
Universidade de São Paulo (USP)
Universidade Federal de São Paulo (UNIFESP)
Resumo An EPR approach to monitor peptide chain aggregation inside resin beads is introduced. Model low and highly peptide-loaded resins containing an aggregating sequence were labeled with a paramagnetic amino acid derivative and studied with regard to their solvation behavior in different solvent systems. for the first time in the peptide synthesis, EPR spectroscopic has allowed the detection of differentiated levels of peptide chain aggregation as a function of solvent and resin loading. (C) 1997, Elsevier B.V. All rights reserved.
Idioma Inglês
Data de publicação 1997-01-27
Publicado em Tetrahedron Letters. Oxford: Pergamon-Elsevier B.V., v. 38, n. 4, p. 517-520, 1997.
ISSN 0040-4039 (Sherpa/Romeo, fator de impacto)
Publicador Elsevier B.V.
Extensão 517-520
Fonte http://dx.doi.org/10.1016/S0040-4039(96)02363-5
Direito de acesso Acesso restrito
Tipo Artigo
Web of Science WOS:A1997WD98800005
Endereço permanente http://repositorio.unifesp.br/handle/11600/25683

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